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KMID : 1059519950390050414
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Journal of the Korean Chemical Society
1995 Volume.39 No. 5 p.414 ~ p.420
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Effective Synthesis of α-Bromo-ω-fluoroalkane with Analysis of Gas-chromatography
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Yu Kook-Hyun
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Abstract
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α-Bromo-ω-fluoroalkanes are synthesized in 19∼55% yields from the reactions of dibromoalkanes with AgF and TBABr in acetonitrile at 82℃ for 20 minutes. The reaction is monitored with gas-chromatography. 1H NMR and 19F NMR-Spectrometer are used for identification of α-bromo-ω-fluoroalkane, difluoroalkane, fluoroalken and bromoalkene.
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